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Appl. Phys. Lett. 45, 615 (1984); doi:10.1063/1.95330 (2 pages)
Formation of bulk metallic glass by fluxing
(Received 21 May 1984; accepted 29 June 1984)
Bulk specimens (0.4–4 g mass) of the alloy Pd40Ni40P20 have been undercooled consistently to the glass state, with no detectable superficial crystallinity, in a molten flux of dehydrated boron oxide. The minimum dimension of the most massive glass specimen, so formed, was 1.0 cm. The absence of crystallinity in the specimens was confirmed by x‐ray diffraction, scanning electron microscopy, and calorimetry.
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A. J. Drehman, A. L. Greer, and D. Turnbull, Appl. Phys. Lett. 41, 716 (1982APPLAB000041000008000716000001).
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