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Appl. Phys. Lett. 97, 171910 (2010); http://dx.doi.org/10.1063/1.3506694 (3 pages)

Resolving ensembled microstructural information of bulk-metallic-glass-matrix composites using synchrotron x-ray diffraction

J. W. Qiao1,2, E. W. Huang3, F. Jiang2, T. Ungár4, G. Csiszár4, L. Li2, Y. Ren5, P. K. Liaw2, and Y. Zhang1

1State Key Laboratory for Advanced Metals and Materials, University of Science and Technology Beijing, Beijing 100083, China
2Department of Materials Science and Engineering, University of Tennessee, Knoxville, Tennessee 37996-2200, USA
3Department of Chemical and Materials Engineering, National Central University, Jhongli, 32001 Taiwan, Republic of China
4Department of Materials Physics, Eötvös University, Budapest H-1518, Hungary
5X-ray Science Division, Argonne National Laboratory, Argonne, Illinois 60439, USA

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(Received 29 August 2010; accepted 6 October 2010; published online 29 October 2010)

The microstructural characterization of the Zr60.0Ti14.7Nb5.3Cu5.6Ni4.4Be10.0 bulk-metallic-glass-matrix composites is investigated using high-energy synchrotron x-ray diffraction. The convoluted diffraction-intensity distribution in the azimuthal direction is naturally yielded from the spatial arrangements of the crystalline dendrites and their amorphous matrix. We facilitate the area selection and the intensity integration of the diffraction collected from a two-dimensional detector to characterize the diffraction intensity of the amorphous matrix. The results enable us to apply the modified Williamson–Hall plots for using the peak width to study the microstrain and micromechanism of the deformation of the crystalline phase.

© 2010 American Institute of Physics

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0003-6951 (print)  
1077-3118 (online)

For access to fully linked references, you need to log in.
    J. W. Qiao, S. Wang, Y. Zhang, P. K. Liaw, and G. L. Chen, Appl. Phys. Lett. 94, 151905 (2009)APPLAB000094000015151905000001.


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